Holodirected coordination sphere around lead(II) in three-dimensional polymeric structure; New precursor for preparation of lead oxide sulfate nano-structures

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dc.contributor.authorAkhbari, Kamran
dc.contributor.authorBeheshti, Saeideh
dc.contributor.authorMorsali, Ali
dc.contributor.authorBüyükgüngör, Orhan
dc.contributor.buuauthorYılmaz, Veysel Turan
dc.contributor.departmentUludağ Üniversitesi/Fen-Edebiyat Fakültesi/Kimya Bölümü.tr_TR
dc.contributor.orcid0000-0002-2849-3332tr_TR
dc.contributor.researcheridL-7238-2018tr_TR
dc.contributor.scopusid7006269202tr_TR
dc.date.accessioned2022-09-09T13:12:55Z
dc.date.available2022-09-09T13:12:55Z
dc.date.issued2014-09-25
dc.description.abstractA new lead(II) three-dimensional coordination polymer, [Pb-2(mu(3)-ANS)(2)(mu(2)-Cl)(2)(H2O)(2)](n) (1) [ANS(-) = 4-amino-1 -naphthalenesulfonateb has been synthesized and characterized. The single-crystal X-ray data of compound 1 shows only one type of Pb-II ion with coordination number of six, the lead atom has distorted octahedral coordination sphere containing stereo-chemically inactive electron lone pair. The thermal stability of 1 was studied by TG-DTA (Thermo gravimetric and differential thermal analyses). Regular morphology of Pb-2(SO4)O nano-particle was prepared from fine powders of compound 1 by calcination process at 700 degrees C. This nano-structure was characterized by XRD (X-ray powder diffraction) and SEM (Scanning electron microscopy).tr_TR
dc.description.sponsorshipUniversity of Tehran (01/1/389845)tr_TR
dc.identifier.citationAkhbari, K. vd. (2014). "Holodirected coordination sphere around lead(II) in three-dimensional polymeric structure; New precursor for preparation of lead oxide sulfate nano-structures". Journal of Molecular Structure, 1074, 279-283.tr_TR
dc.identifier.endpage283tr_TR
dc.identifier.issn0022-2860
dc.identifier.issn1872-8014
dc.identifier.scopus2-s2.0-84903744929tr_TR
dc.identifier.startpage279tr_TR
dc.identifier.urihttps://doi.org/10.1016/j.molstruc.2014.06.004
dc.identifier.urihttps://www.sciencedirect.com/science/article/pii/S0022286014006000
dc.identifier.urihttp://hdl.handle.net/11452/28619
dc.identifier.volume1074tr_TR
dc.identifier.wos000340315200035
dc.indexed.scopusScopustr_TR
dc.indexed.wosSCIEtr_TR
dc.language.isoentr_TR
dc.publisherElseviertr_TR
dc.relation.collaborationYurt içitr_TR
dc.relation.collaborationYurt dışıtr_TR
dc.relation.journalJournal of Molecular Structuretr_TR
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergitr_TR
dc.rightsinfo:eu-repo/semantics/closedAccesstr_TR
dc.subjectLead(II)tr_TR
dc.subjectCoordination polymertr_TR
dc.subjectHolodirectedtr_TR
dc.subjectLead oxide sulfatetr_TR
dc.subjectNano-particletr_TR
dc.subjectDesigntr_TR
dc.subjectRoomtr_TR
dc.subjectChemistrytr_TR
dc.subjectDifferential thermal analysistr_TR
dc.subjectLeadtr_TR
dc.subjectLead oxidetr_TR
dc.subjectNanoparticlestr_TR
dc.subjectScanning electron microscopytr_TR
dc.subjectX ray powder diffractiontr_TR
dc.subjectCoordination numbertr_TR
dc.subjectCoordination polymerstr_TR
dc.subjectCoordination spheretr_TR
dc.subjectElectron lone pairtr_TR
dc.subjectHolodirectedtr_TR
dc.subjectOctahedral coordinationtr_TR
dc.subjectPolymeric structurestr_TR
dc.subjectThermo-gravimetrictr_TR
dc.subjectPolymerstr_TR
dc.subject.scopusCoordination Polymer; X-Ray Powder Diffraction; Elemental Analysestr_TR
dc.subject.wosChemistry, physicaltr_TR
dc.titleHolodirected coordination sphere around lead(II) in three-dimensional polymeric structure; New precursor for preparation of lead oxide sulfate nano-structurestr_TR
dc.typeArticle
dc.wos.quartileQ3tr_TR

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