Synthesis of PbO nano-particles from a new one-dimensional lead(II) coordination polymer precursor

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dc.contributor.authorSadeghzadeh, Homa
dc.contributor.authorMorsali, Ali
dc.contributor.authorBüyükgüngör, Orhan
dc.contributor.buuauthorYılmaz, Veysel Turan
dc.contributor.departmentUludağ Üniversitesi/Fen-Edebiyat Fakültesi/Kimya Bölümü.tr_TR
dc.contributor.orcid0000-0002-2849-3332tr_TR
dc.contributor.researcheridL-7238-2018tr_TR
dc.contributor.scopusid7006269202tr_TR
dc.date.accessioned2021-12-02T08:30:34Z
dc.date.available2021-12-02T08:30:34Z
dc.date.issued2010-04-15
dc.description.abstractA new Pb(II) one-dimensional coordination polymer, [Pb(mu-NO2)(mu-pyc)(H2O)](n) (1). Hpyc = 2-pyridine-carboxylic acid] was prepared and characterized by elemental analyses, powder XRD diffraction and IR spectroscopy. Compound 1 was structurally characterized by single-crystal X-ray diffraction and one-dimensional coordination polymer with coordination environment of PbNO6. The thermal stability of compound 1 showed that compound 1 decomposes at 110-500 degrees C and the final product is PbO. This polymeric precursor has been used to make PbO nano-particles using two different surfactants. The new nano-structure was characterized by scanning electron microscopy and X-ray powder diffraction. This study demonstrates that the coordination polymers may be suitable precursors for the preparation of nanoscale materials.en_US
dc.description.sponsorshipTarbiat Modares Universityen_US
dc.identifier.citationSadeghzadeh, H. vd. (2010). "Synthesis of PbO nano-particles from a new one-dimensional lead(II) coordination polymer precursor". Materials Letters, 64(7), 810-813.en_US
dc.identifier.endpage813tr_TR
dc.identifier.issn0167-577X
dc.identifier.issn1873-4979
dc.identifier.issue7tr_TR
dc.identifier.scopus2-s2.0-76849101386tr_TR
dc.identifier.startpage810tr_TR
dc.identifier.urihttps://doi.org/10.1016/j.matlet.2010.01.017
dc.identifier.urihttps://www.sciencedirect.com/science/article/pii/S0167577X10000297
dc.identifier.urihttp://hdl.handle.net/11452/22947
dc.identifier.volume64tr_TR
dc.identifier.wos000276190100005
dc.indexed.scopusScopusen_US
dc.indexed.wosSCIEen_US
dc.language.isoenen_US
dc.publisherElsevieren_US
dc.relation.collaborationYurt içitr_TR
dc.relation.collaborationYurt dışıtr_TR
dc.relation.journalMaterials Lettersen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergitr_TR
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectCrystal structureen_US
dc.subjectThermal propertiesen_US
dc.subjectNano-materialsen_US
dc.subjectCoordination reactionsen_US
dc.subjectDiffractionen_US
dc.subjectLeaden_US
dc.subjectLead oxideen_US
dc.subjectMaterials propertiesen_US
dc.subjectNanoparticlesen_US
dc.subjectScanning electron microscopyen_US
dc.subjectSurface active agentsen_US
dc.subjectThermodynamic stabilityen_US
dc.subjectX ray diffractionen_US
dc.subjectX ray powder diffractionen_US
dc.subjectCoordination environmenten_US
dc.subjectCoordination polymersen_US
dc.subjectElemental analysisen_US
dc.subjectIR spectroscopyen_US
dc.subjectNano-materialsen_US
dc.subjectNano-scale materialsen_US
dc.subjectOne-dimensional coordination polymeren_US
dc.subjectPolymeric precursorsen_US
dc.subjectPowder XRDen_US
dc.subjectSingle crystal x-ray diffractionen_US
dc.subjectThermal propertiesen_US
dc.subjectThermal stabilityen_US
dc.subject.scopusMetal-Organic Frameworks; X-Ray Powder Diffraction; Elemental Analysesen_US
dc.subject.wosMaterials science, multidisciplinaryen_US
dc.subject.wosPhysics, applieden_US
dc.titleSynthesis of PbO nano-particles from a new one-dimensional lead(II) coordination polymer precursoren_US
dc.typeArticle
dc.wos.quartileQ1 (Materials science, multidisciplinary)en_US
dc.wos.quartileQ2 (Physics, applied)en_US

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